9/3/2019 Tablecurve 2d V5 01 Crack Cocaine
.Cagliostro, D. E.; Lerner, N. (Inventor)1983-01-01This invention relates to a method of carbonizing polyacrylonitrile fibers by exposing the fibers at an elevated temperature to an oxidizing atmosphere; then exposing the oxidized fibers to an atmosphere of an inert gas such as nitrogen containing a carbonaceous material such as acetylene. The fibers are preferably treated with an organic compound, for example benzoic acid, before the exposure to an oxidizing atmosphere. The invention also relates to the resulting fibers. The treated fibers have enhanced tensile strength.Hiremath, Nitilaksha; Evora, Maria Cecilia; Naskar, Amit K.2017-07-31For the first time, uniform distribution of surface functionalized carbon nanofibers (CNFs) has been achieved in low molecular weight (≈120,000 g/mol) textile grade- polyacrylonitrile ( PAN)-based composite filaments. Furthermore, surface grafting of CNFs with acrylonitrile enhances the dispersion of nanofibers in PAN fiber matrix.
XPS study reveals high atomic nitrogen content (7%) on the CNF surface due to the grafting reaction. The solution-spun filaments have been characterized for distribution of CNFs in the PAN matrix by electron microscopy. PAN composite filaments containing 3.2 wt.% CNF and processed at draw ratio of ≈6.3 exhibit enhanced tensile strength and modulus by more than threemore » folds compared to the control PAN filament. Because of chemically compatible surface modification of the nanofibers, better dispersion and improved mechanical properties were accomplished in the reinforced PAN fibers. This should then allow the production of CNF reinforced carbon fibers with improved tensile properties. An increase in CNF loading (6.4 wt.%), however, reduced performance due to inefficient alignment of CNF along the fiber axis. Nevertheless, hot stretching (at draw ratio ≈ 10) of the filaments enhanced tensile strength and elastic modulus of PAN composite filaments by 20–30% compared to the control hot stretched PAN filaments.« less.Hiremath, Nitilaksha; Evora, Maria Cecilia; Naskar, Amit K.For the first time, uniform distribution of surface functionalized carbon nanofibers (CNFs) has been achieved in low molecular weight (≈120,000 g/mol) textile grade- polyacrylonitrile ( PAN)-based composite filaments.
Furthermore, surface grafting of CNFs with acrylonitrile enhances the dispersion of nanofibers in PAN fiber matrix. XPS study reveals high atomic nitrogen content (7%) on the CNF surface due to the grafting reaction. The solution-spun filaments have been characterized for distribution of CNFs in the PAN matrix by electron microscopy. PAN composite filaments containing 3.2 wt.% CNF and processed at draw ratio of ≈6.3 exhibit enhanced tensile strength and modulus by more than threemore » folds compared to the control PAN filament. Because of chemically compatible surface modification of the nanofibers, better dispersion and improved mechanical properties were accomplished in the reinforced PAN fibers.
This should then allow the production of CNF reinforced carbon fibers with improved tensile properties. An increase in CNF loading (6.4 wt.%), however, reduced performance due to inefficient alignment of CNF along the fiber axis. Nevertheless, hot stretching (at draw ratio ≈ 10) of the filaments enhanced tensile strength and elastic modulus of PAN composite filaments by 20–30% compared to the control hot stretched PAN filaments.« less.Zhao, Rui-Xue; Sun, Peng-fei; Liu, Rui-jian; Ding, Zhan-hui; Li, Xiang-shan; Liu, Xiao-yang; Zhao, Xu-dong; Gao, Zhong-min2018-03-01The stabilized polyacrylonitrile ( PAN) fibers were obtained after heating the precursor PAN fibers under air atmosphere by different procedures. The surface structures and compositions of as-prepared stabilized PAN fibers have been investigated by SEM, SSNMR, XPS and Raman spectroscopy.
The results show that 200 °C, 220 °C, 250 °C, and 280 °C are key temperatures for the preparation of stabilized PAN fibers. The effect of heating gradient on the structure of stabilized PAN fibers has been studied. The possible chemical structural formulas for the PAN fibers is provided, which include the stable and unstable structure. The stable structure (α-type) could endure the strong chemical reactions and the unstable structure (β- or γ-type) could mitigate the drastic oxidation reactions.
The inferences of chemical formula of stabilized PAN fibers are benefit to the design of appropriate surface structure for the production for high quality carbon fibers.Bakar, S. C.; Eleyas, A.; Nazeri, M. M.2018-03-01Currently, electrospinning is a very famous technique and widely used for forming polymer nanofibers. In this paper, the Polyacrylonitrile ( PAN) nanofibers were prepared in concentration of 10wt% with varied processing parameters that can affect the properties of PAN fiber in term of fiber diameter and electrical conductivity was presented. Voltage of 10, 15 and 20 kV with PAN flow rate of 1 electrospun PAN fibers were then undergo pyrolysis at 800°C for 30 minutes.
The resultant PAN nanofibers were then analysed by SEM, XRD and four point probe test after pyrolysis process. SEM image show continuos uniform and smooth surface fibrous structure of electrospun PAN fibers with average diameter of 1.81 μm. The fiber morphology is controlled by manipulating the processing parameters of electrospinning process. The results showed that the resistance of electrospun PAN fibers decreases as the processing parameter changes by increasing the applied voltage and flow rate of electrospinning.Gonzalez, Mark A.; Walter, Wayne W.2014-03-01A polymer-based nanofiber composite actuator designed for contractile actuation was fabricated by electrospinning, stimulated by electrolysis, and characterized by electrochemical and mechanical testing to address performance limitations and understand the activation processing effects on actuation performance. Currently, Electroactive polymers (EAPs) have provided uses in sensory and actuation technology, but have either low force output or expand rather than contract, falling short in capturing the natural kinetics and mechanics of muscle needed to provide breakthroughs in the bio-medical and robotic fields. In this study, activated Polyacrylonitrile ( PAN) fibers have demonstrated biomimetic functionalities similar to the sarcomere contraction responsible for muscle function. Activated PAN has also been shown to contract and expand by electrolysis when in close vicinity to the anode and cathode, respectively.
PAN nanofibers (500 nm) especially show faster response to changes in environmental pH and improved mechanical properties compared to larger diameter fibers. Tensile testing was conducted to examine changes in mechanical properties between annealing and hydrolysis processing. Voltage driven transient effects of localized pH were examined to address pHdefined actuation thresholds of PAN fibers. Electrochemical contraction rates of the PAN/Graphite composite actuator demonstrated up to 25%/min. Strains of 58.8%, ultimate stresses up to 77.1 MPa, and moduli of 0.21 MPa were achieved with pure PAN nanofiber mats, surpassing mechanical properties of natural muscles. Further improvements, however, to contraction rates and Young's moduli were found essential to capture the function and performance of skeletal muscles appropriately.Liu, Wanwan; Jin, Yang; Wang, Yangyi; Ge, Mingqiao; Gao, Qiang2017-12-01In this work, conductive polyacrylonitrile ( PAN) composite fiber with thermosensitive property was successfully prepared via wet-spinning.
Thermochromic pigment (TCP) microsphere capsules were applied to manufacture color-changing fibers. Meanwhile, light-colored conductive whiskers (ATO@TiO2) were employed to endow polyacrylonitrile fibers with conductivity without prejudicing their thermosensitive property. Interestingly, unlike other conductive fibers in dark color, this kind of conductive composite fiber can be dyed by thermosensitive pigment. The obtained composite fiber containing 20 vol% ATO@TiO2 whiskers shows a resistivity of 105 Ω cm and could generate heat by Joule heating when being applied under a certain voltage. The composite fiber shows a red color at room temperature, while the color of the composite fiber fades gradually and finally becomes white as temperature rise. This simple and cost-effective approach is expected to inspire more research into the applications of multifunctional conductive fibers.Cherry, De'Andre JamesPhase change materials (PCMs) are generally substances with a high heat of fusion in the process of solid to liquid phase change. The nature of PCMs make them efficient materials to store and retrieve large amounts of thermal energy.
Presently, high efficiency thermal energy storage/retrieval in applications where flexibility and space saving are required, such as smart textiles, still remains as a challenge. In this study, lauric acid (LA) and myristic acid (MA) were combined to prepare a specific binary fatty acid eutectic (LA-MA) with a melting point near the operating body temperature of a human being and then encapsulated in polyacrylonitrile ( PAN) nanofibers through the electrospinning technique.
Functionalized PCM-enhanced PAN nanofibers containing LA-MA at 30%, 50%, 70% and 100% of the weight of the PAN were successfully synthesized. The morphological structures and thermal energy storage capacity of the PCM-enhanced PAN nanofibers were characterized by electron microscopy (EM) and differential scanning calorimetry (DSC). The novel PCM-enhanced PAN nanofibers maintained their cylindrical fiber morphology after multiple heating-cooling cycles and retained their latent heat storage functionality.
Thus, it is envisioned that the prepared PCM-enhanced PAN nanofibers will find use in applications such as smart textiles where temperature regulation functionality is required.Li, Xiang; Qin, Aiwen; Zhao, Xinzhen; Liu, Dapeng; Wang, Haiye; He, Chunju2015-09-14Drawing to change the structural properties and cyclization behaviors of the polyacrylonitrile ( PAN) chains in crystalline and amorphous regions is carried out on PAN and PAN/carbon nanotube (CNT) composite fibers. Various characterization methods including Fourier transform infrared spectroscopy, differential scanning calorimetry, X-ray diffraction and thermal gravimetric analysis are used to monitor the structural evolution and cyclization behaviors of the fibers. With an increase of the draw ratio during the plasticized spinning process, the structural parameters of the fibers, i.e. Crystallinity and planar zigzag conformation, are decreased at first, and then increased, which are associated with the heat exchange rate and the oriented-crystallization rate. A possible mechanism for plasticized spinning is proposed to explain the changing trends of crystallinity and planar zigzag conformation.
PAN and PAN/CNT fibers exhibit various cyclization behaviors induced by drawing, e.g., the initiation temperature for the cyclization (Ti) of PAN fibers is increased with increasing draw ratio, while Ti of PAN/CNT fibers is decreased. Drawing also facilitates cyclization and lowers the percentage of β-amino nitrile for PAN/CNT fibers during the stabilization.Gonzalez, Mark A.A polymer-based nanofiber composite actuator designed for linear actuation was fabricated by electrospinning, actuated by electrolysis, and characterized by electrical and mechanical testing to address performance limitations and understand the activation processing effects on actuation performance. Currently, Electroactive polymers (EAPs) have provided uses in sensory and actuation technology, but have either low force output or expand rather than contract, falling short in capturing the natural motion and function of muscle desperately needed to provide breakthroughs in the bio-medical and robotic fields. Previous research has shown activated Polyacrylonitrile ( PAN) fibers having biomimetic functionalities similar to the sarcomere contraction responsible for muscle function. Activated PAN is also known to contract and expand by electrolysis when in close vicinity to the anode and cathode, respectively.
PAN nanofibers especially show faster response to changes in environmental pH and improved mechanical properties over larger diameter fibers. Conductive additives were introduced to the electrospinning solution and activated in an attempt to create composite PAN nanofiber gel actuators with improved conductivity and eliminate the need of stiff electrodes.
Tensile testing was conducted to examine changes in mechanical properties between annealing and hydrolysis processing. Introducing conductive additives did not show a significant increase in conductivity and created unusable samples, requiring alternative electrode materials. Electrochemical contraction rates up to 25%/ min were achieved.
Strains of 58.8%, ultimate stresses up to 77.1 MPa, and moduli of 0.21 MPa were achieved with pure PAN nanofiber mats, surpassing mechanical properties of natural muscles. Improvements to contraction rates and young's moduli are necessary to capture the function and performance of skeletal muscles properly.Morris, E. Ashley; Weisenberger, Matthew C.; Abdallah, Mohamed G.In this study, carbon fibers are unique reinforcing agents for lightweight composite materials due to their outstanding mechanical properties and low density. Current technologies are capable of producing carbon fibers with 90-95% of the modulus of perfect graphite (1025 GPa).
However, these same carbon fibers possess less than 10% of the theoretical carbon fiber strength, estimated to be about 100 GPa.1 Indeed, attempts to increase carbon fiber rigidity results in lower breaking strength. To develop advanced carbon fibers with both very high strength and modulus demands a new manufacturing methodology. Here, we report a method of manufacturing high strength, verymore » high modulus carbon fibers from a very high molecular weight (VHMW) polyacrylonitrile ( PAN) precursor without the use of nanomaterial additives such as nucleating or structure-templating agents, as have been used by others.2,3« less.Morris, E.
Ashley; Weisenberger, Matthew C.; Abdallah, Mohamed G.2016-02-02In this study, carbon fibers are unique reinforcing agents for lightweight composite materials due to their outstanding mechanical properties and low density. Current technologies are capable of producing carbon fibers with 90-95% of the modulus of perfect graphite (1025 GPa). However, these same carbon fibers possess less than 10% of the theoretical carbon fiber strength, estimated to be about 100 GPa.1 Indeed, attempts to increase carbon fiber rigidity results in lower breaking strength. To develop advanced carbon fibers with both very high strength and modulus demands a new manufacturing methodology. Here, we report a method of manufacturing high strength, verymore » high modulus carbon fibers from a very high molecular weight (VHMW) polyacrylonitrile ( PAN) precursor without the use of nanomaterial additives such as nucleating or structure-templating agents, as have been used by others.2,3« less.Xie, Yujia; Liu, Xiaoxing; Tao, Minli2016-01-01A multistep experiment for a synthesis laboratory course that incorporates topics in organic synthesis, chemical analysis, and instrumental analysis was developed. Students prepared a tertiaryamine-functionalized polyacrylonitrile fiber ( PANsubscript TF), and it was subsequently utilized as an immobilized catalyst in a three-component.Park, Sejoon; Yoo, Seung Hwa; Kang, Ha Ri; Jo, Seong Mu; Joh, Han-Ik; Lee, Sungho2016-01-01An electron beam was irradiated on polyacrylonitrile ( PAN) fibers prior to thermal stabilization.
The electron-beam irradiation effectively shortened the thermal stabilization process by one fourth compared with the conventional thermal stabilization process. A comprehensive mechanistic study was conducted regarding this shortening of the thermal stabilization by electron-beam irradiation. Various species of chain radicals were produced in PAN fibers by electron-beam irradiation and existed for a relatively long duration, as observed by electron spin resonance spectroscopy. Subsequently, these radicals were gradually oxidized to peroxy radicals in the presence of oxygen under storage or heating. We found that these peroxy radicals (CO) enabled such an effective shortcut of thermal stabilization by acting as intermolecular cross-linking and partial aromatization points in the low temperature range (100–130 °C) and as earlier initiation seeds of successive cyclization reactions in the next temperature range (130–140 °C) of thermal stabilization.
Finally, even at a low irradiation dose (200 kGy), followed by a short heat treatment (230 °C for 30 min), the PAN fibers were sufficiently stabilized to produce carbon fibers with tensile strength and modulus of 2.3 and 216 GPa, respectively, after carbonization. PMID:27349719.Jain, Swati; Chattopadhyay, Sruti; Jackeray, Richa; Zainul Abid, C K V; Kumar, Manoj; Singh, Harpal2010-10-15Accurate determination of concentration of immunoglobulin (IgG) to tetanus toxoid is important in order to evaluate the immunogenicity of tetanus toxoid vaccines, immune competence in individual patients and to measure the prevalence of immunity in populations. Surface modified polyacrylonitrile ( PAN) fibers were evaluated as a matrix to develop highly sensitive method for the detection of anti-tetanus antibody in a sandwich ELISA format.
In the proposed method tetanus toxoid immobilized on modified PAN fibers was used to detect anti-tetanus antibody (raised in horse hence represented as horse anti-tetanus toxoid or HAT-Ab) with horse raddish peroxidase enzyme conjugated with Rabbit anti-Horse IgG (RAH-HRP) as the label within 2.5h. A sigmoidal pattern for the detection of different concentration of antibody ranging from 1.0 to 0.0001 IU mL(-1) was validated. The immunoassay recorded a very high sensitivity as concentration as low as 0.0005 IU mL(-1) of HAT-Ab was detected. The intra- and inter-assay precision for 3 parallel measurements of 0.01 and for 0.001 IU mL(-1) of antibody varied from 5.4% to 11% and 5.7% to 20% respectively. PAN fibers were also used to qualitatively access the presence of different level of anti-tetanus antibody spiked in human blood. Seroepidemiological studies to measure the immunity against tetanus were conducted with twenty-five human beings belonging to various age groups using modified PAN-ELISA. The sensitivity, specificity and the reproducibility of the developed immunoassay indicate the potential application of modified PAN fibers in the field of immunodiagnostics.
Copyright © 2010 Elsevier B.V. All rights reserved.Durable antibacterial Ag/ polyacrylonitrile (Ag/ PAN) hybrid nanofibers were prepared by atmospheric plasma treatment and electrospinning. Atmospheric helium plasma treatment was first used to reduce the silver nitrate precursor in pre-electrospinning solutions into metallic silver nanoparticles, foll.Liang, Yinzheng; Ji, Liwen; Guo, Bingkun; Lin, Zhan; Yao, Yingfang; Li, Ying; Alcoutlabi, Mataz; Qiu, Yiping; Zhang, XiangwuLithium lanthanum titanate oxide (LLTO)/ polyacrylonitrile ( PAN) submicron composite fiber-based membranes were prepared by electrospinning dispersions of LLTO ceramic particles in PAN solutions. These ionic-conducting LLTO/ PAN composite fiber-based membranes can be directly used as lithium-ion battery separators due to their unique porous structure. Ionic conductivities were evaluated after soaking the electrospun LLTO/ PAN composite fiber-based membranes in a liquid electrolyte, 1 M lithium hexafluorophosphate (LiPF 6) in ethylene carbonate (EC)/ethyl methyl carbonate (EMC) (1:1 vol).
It was found that, among membranes with various LLTO contents, 15 wt.% LLTO/ PAN composite fiber-based membranes provided the highest ionic conductivity, 1.95 × 10 -3 S cm -1. Compared with pure PAN fiber membranes, LLTO/ PAN composite fiber-based membranes had greater liquid electrolyte uptake, higher electrochemical stability window, and lower interfacial resistance with lithium.
In addition, lithium//1 M LiPF 6/EC/EMC//lithium iron phosphate cells containing LLTO/ PAN composite fiber-based membranes as the separator exhibited high discharge specific capacity of 162 mAh g -1 and good cycling performance at 0.2 C rate at room temperature.Wang, Yanqing; Fugetsu, Bunshi; Wang, Zhipeng; Gong, Wei; Sakata, Ichiro; Morimoto, Shingo; Hashimoto, Yoshio; Endo, Morinobu; Dresselhaus, Mildred; Terrones, Mauricio2017-01-01Nitrogen-doped porous activated carbon monoliths (NDP-ACMs) have long been the most desirable materials for supercapacitors. Unique to the conventional template based Lewis acid/base activation methods, herein, we report on a simple yet practicable novel approach to production of the three-dimensional NDP-ACMs (3D-NDP-ACMs). Polyacrylonitrile ( PAN) contained carbon nanotubes (CNTs), being pre-dispersed into a tubular level of dispersions, were used as the starting material and the 3D-NDP-ACMs were obtained via a template-free process. First, a continuous mesoporous PAN/CNT based 3D monolith was established by using a template-free temperature-induced phase separation (TTPS). Second, a nitrogen-doped 3D-ACM with a surface area of 613.8 m2/g and a pore volume 0.366 cm3/g was obtained.
A typical supercapacitor with our 3D-NDP-ACMs as the functioning electrodes gave a specific capacitance stabilized at 216 F/g even after 3000 cycles, demonstrating the advantageous performance of the PAN/CNT based 3D-NDP-ACMs. PMID:28074847.Wang, Yanqing; Fugetsu, Bunshi; Wang, Zhipeng; Gong, Wei; Sakata, Ichiro; Morimoto, Shingo; Hashimoto, Yoshio; Endo, Morinobu; Dresselhaus, Mildred; Terrones, Mauricio2017-01-01Nitrogen-doped porous activated carbon monoliths (NDP-ACMs) have long been the most desirable materials for supercapacitors. Unique to the conventional template based Lewis acid/base activation methods, herein, we report on a simple yet practicable novel approach to production of the three-dimensional NDP-ACMs (3D-NDP-ACMs). Polyacrylonitrile ( PAN) contained carbon nanotubes (CNTs), being pre-dispersed into a tubular level of dispersions, were used as the starting material and the 3D-NDP-ACMs were obtained via a template-free process. First, a continuous mesoporous PAN/CNT based 3D monolith was established by using a template-free temperature-induced phase separation (TTPS). Second, a nitrogen-doped 3D-ACM with a surface area of 613.8 m2/g and a pore volume 0.366 cm3/g was obtained. A typical supercapacitor with our 3D-NDP-ACMs as the functioning electrodes gave a specific capacitance stabilized at 216 F/g even after 3000 cycles, demonstrating the advantageous performance of the PAN/CNT based 3D-NDP-ACMs.Wang, Yanqing; Fugetsu, Bunshi; Wang, Zhipeng; Gong, Wei; Sakata, Ichiro; Morimoto, Shingo; Hashimoto, Yoshio; Endo, Morinobu; Dresselhaus, Mildred; Terrones, Mauricio2017-01-11Nitrogen-doped porous activated carbon monoliths (NDP-ACMs) have long been the most desirable materials for supercapacitors.
Unique to the conventional template based Lewis acid/base activation methods, herein, we report on a simple yet practicable novel approach to production of the three-dimensional NDP-ACMs (3D-NDP-ACMs). Polyacrylonitrile ( PAN) contained carbon nanotubes (CNTs), being pre-dispersed into a tubular level of dispersions, were used as the starting material and the 3D-NDP-ACMs were obtained via a template-free process. First, a continuous mesoporous PAN/CNT based 3D monolith was established by using a template-free temperature-induced phase separation (TTPS). Second, a nitrogen-doped 3D-ACM with a surface area of 613.8 m 2 /g and a pore volume 0.366 cm 3 /g was obtained. A typical supercapacitor with our 3D-NDP-ACMs as the functioning electrodes gave a specific capacitance stabilized at 216 F/g even after 3000 cycles, demonstrating the advantageous performance of the PAN/CNT based 3D-NDP-ACMs.Li, Zhaohua; Dai, Wenjing; Yu, Lihong; Liu, Le; Xi, Jingyu; Qiu, Xinping; Chen, Liquan2014-11-12Acid-base blend membrane prepared from sulfonated poly(ether ether ketone) (SPEEK) and polyacrylonitrile ( PAN) was detailedly evaluated for vanadium redox flow battery (VRFB) application. SPEEK/ PAN blend membrane exhibited dense and homogeneous cross-section morphology as scanning electron microscopy and energy-dispersive X-ray spectroscopy images show.
The acid-base interaction of ionic cross-linking and hydrogen bonding between SPEEK and PAN could effectively reduce water uptake, swelling ratio, and vanadium ion permeability, and improve the performance and stability of blend membrane. Because of the good balance of proton conductivity and vanadium ion permeability, blend membrane with 20 wt% PAN (S/ PAN-20%) showed higher Coulombic efficiency (96.2% vs 91.1%) and energy efficiency (83.5% vs 78.4%) than Nafion 117 membrane at current density of 80 mA cm(-2) when they were used in VRFB single cell. Besides, S/ PAN-20% membrane kept a stable performance during 150 cycles at current density of 80 mA cm(-2) in the cycle life test. Hence the SPEEK/ PAN acid-base blend membrane could be used as promising candidate for VRFB application.Kampalanonwat, Pimolpun; Supaphol, Pitt2010-12-01Polyacrylonitrile ( PAN) nanofiber mats were prepared by electrospinning and they were further modified to contain amidino diethylenediamine chelating groups on their surface via heterogeneous reaction with diethylenetriamine (DETA).
The obtained aminated PAN (APAN) nanofiber mats were evaluated for their chelating property with four types of metal ions, namely Cu(II), Ag(I), Fe(II), and Pb(II) ions. The amounts of the metal ions adsorbed onto the APAN nanofiber mats were influenced by the initial pH and the initial concentration of the metal ion solutions. Increasing the contact time also resulted in a monotonous increase in the adsorbed amounts of the metal ions, which finally reached equilibria at about 10 h for Cu(II) ions and about 5 h for Ag(I), Fe(II), and Pb(II) ions.
The maximal adsorption capacities of the metal ions on the APAN nanofiber mats, as calculated from the Langmuir model, were 150.6, 155.5, 116.5, and 60.6 mg g(-1), respectively. Lastly, the spent APAN nanofiber mats could be facilely regenerated with a hydrochloric acid (HCl) aqueous solution.Jiao, Fei; Zhang, Fengjiao; Zang, Yaping; Zou, Ye; Di, Chong'an; Xu, Wei; Zhu, Daoben2014-03-04Ultrathin carbon films were prepared by carbonization of a solution processed polyacrylonitrile ( PAN) film in a moderate temperature range (500-700 °C). The films displayed balanced hole (0.50 cm(2) V(-1) s(-1)) and electron mobilities (0.20 cm(2) V(-1) s(-1)) under ambient conditions. Spectral characterization revealed that the electrical transport is due to the formation of sp(2) hybridized carbon during the carbonization process. A CMOS-like inverter demonstrated the potential application of this material in the area of carbon electronics, considering its processability and low-cost.Gan, Yong X.; Panahi, Niousha; Yu, Christina; Gan, Jeremy B.; Cheng, Wanli2018-05-01Red light-emitting polymeric micro- and nanofibers were made by electrohydrodynamic co-casting of two fluids. One fluid contains a 10 wt% concentration europium (III) complex dissolved in a dimethylformamide (DMF) solvent. The europium complex, an Eu3+ compound with the nominal formula of Eu(BA)3phen/ PAN, consists of polyacrylonitrile ( PAN), 1,10-phenanthroline (phen), and benzoic acid (BA).
The other fluid consists of iron metal oxide nanoparticles dispersed in a solution containing 10 wt% polyacrylonitrile polymer in DMF solvent. The two fluids were electrohydrodynamically co-cast onto a soft tissue paper using a stainless steel coaxial nozzle.
The intensity of the electric field used for the co-casting was 1.5 kV/cm. Scanning electron microscopic observation on the fibers obtained from the co-casting was made. The size of the fibers ranges from several hundreds of nanometers to several microns. Energy dispersive X-ray spectroscopic analysis of the fibers confirmed that the major elements included C, O, Fe, and Eu. The fluorescence of the two types of fibers was tested under the excitation of a UV light source.
It was found that when the europium complex-containing solution was the sheath fluid and the iron-containing solution was the core, the prepared fibers showed red light-emitting behavior under ultraviolet light. Time-dependent fluorescence shows the two-stage decaying behavior. The first stage lasts about 2000 s and the intensity of fluorescence decreases linearly. The second stage reveals the slow decaying behavior and it lasts longer than 3 h.
Based on the bi-exponential data fitting using a processing MATLAB code, the fluorescence-related constants were extracted. A bi-exponential formula was proposed to describe the time-dependent fluorescence behavior of the fiber made by the europium complex-containing solution as the sheath fluid. The decaying in the fluorescence shows two different stages.
The first stage lasts about 2000 s and it is characterized.Kamran Sami, Syed; Siddiqui, Saqib; Tajmeel Feroze, Muhammad; Chung, Chan-Hwa2017-11-01To pursue high-performance energy storage devices with both high energy density and power density, one-dimensional (1D) nanostructures play a key role in the development of functional devices including energy conversion, energy storage, and environmental devices. The polyacrylonitrile ( PAN) nanofibers were obtained by the versatile electrospinning method. An ultra-thin nickel-cobalt sulfide (NiCoS) layer was conformably electrodeposited on a self-standing PAN nanofibers by cyclic voltammetry to fabricate the light-weighted porous electrodes for supercapacitors. The porous web of PAN nanofibers acts as a high-surface-area scaffold with significant electrochemical performance, while the electrodeposition of metal sulfide nanosheet further enhances the specific capacitance.
The fabricated NiCoS on PAN (NiCoS/ PAN) nanofibers exhibits a very high capacitance of 1513 F g-1 at 5 A g-1 in 1 M potassium chloride (KCl) aqueous electrolyte with superior rate capability and excellent electrochemical stability as a hybrid electrode. The high capacitance of the NiCoS is attributed to the large surface area of the electrospun PAN nanofibers scaffold, which has offered a large number of active sites for possible redox reaction of ultra-thin NiCoS layer. Benefiting from the compositional features and electrode architectures, the hybrid electrode of NiCoS/ PAN nanofibers shows greatly improved electrochemical performance with an ultra-high capacitance (1124 F g-1 at 50 A g-1).Chen, Si Cong; Su, Jincai; Fu, Feng-Jiang; Mi, Baoxia; Chung, Tai-Shung2013-01-01We have examined the gypsum (CaSO42H2O) scaling phenomena on membranes with different physicochemical properties in forward osmosis (FO) processes. Three hollow fiber membranes made of (1) cellulose acetate (CA), (2) polybenzimidazole (PBI)/polyethersulfone (PES) and (3) PBI-polyhedral oligomeric silsesquioxane (POSS)/ polyacrylonitrile ( PAN) were studied. For the first time in FO processes, we have found that surface ionic interactions dominate gypsum scaling on the membrane surface.
A 70% flux reduction was observed on negatively charged CA and PBI membrane surfaces, due to strong attractive forces. The PBI membrane surface also showed a slightly positive charge at a low pH value of 3 and exhibited a 30% flux reduction. The atomic force microscopy (AFM) force measurements confirmed a strong repulsive force between gypsum and PBI at a pH value of 3. The newly developed PBI-POSS/ PAN membrane had ridge morphology and a contact angle of 51.42° ± 14.85° after the addition of hydrophilic POSS nanoparticles and 3 min thermal treatment at 95 °C. Minimal scaling and an only 1.3% flux reduction were observed at a pH value of 3. Such a ridge structure may reduce scaling by not providing a locally flat surface to the crystallite at a pH value of 3; thus, gypsum would be easily washed away from the surface. PMID:24957062.Ren, Dongxia; Sun, Chengjun; Ma, Guanqun; Yang, Danni; Zhou, Chen; Xie, Jiayu; Li, Yongxin2018-01-01A new method has been developed to simultaneously determine 7 pyrethroid residues in tea brew using gas chromatography-mass spectrometry (GC-MS) combined with solid phase microextraction (SPME) with multiwalled carbon nanotubes (MWCNTs) coated fiber.
The MWCNTs coated fiber of SPME was homemade by using stainless steel wire as coating carrier and polyacrylonitrile ( PAN) solution as adhesive glue. Under the optimized conditions, a good linearity was shown for bifenthrin, fenpropathrin, permethrin, and cyfluthrin in 1-50 ng mL -1 and for cypermethrin, fenvalerate, and deltamethrin in 5-50 ng mL -1. The correlation coefficients were in the range of 0.9948-0.9999.
The average recoveries of 7 pyrethroids were 94.2%-107.3% and the relative standard deviations (RSDs) were less than 15%. The detection limit of the method ranged from 0.12 to 1.65 ng mL -1. The tea brew samples made from some commercial tea samples were analyzed.
Among them, bifenthrin, fenpropathrin, and permethrin were found. The results show that the method is rapid and sensitive and requires low organic reagent consumption, which can be well used for the detection of the pyrethroids in tea brew.Liu, Chunyi; Li, Xiang; Ma, Bomou; Qin, Aiwen; He, Chunju2014-12-01The functionalizing nanoporous polyacrylonitrile-based oxidized membrane ( PAN-OM) firmly immobilized with highly reactive nanoscale zero-valent iron (NZVI) are successfully prepared via an innovative in situ synthesis method. Due to the formation of ladder structure, the PAN-OM present excellent thermal and chemical stabilities as a new carrier for the in-situ growth of NZVI via firm chelation and reduction action, respectively, which prevent the aggregation and release of NZVI.
The developed NZVI-immobilized membrane present effective decolorizing efficiency to both anionic methyl blue and cationic methylene blue with a pseudo-first-order decay and degrading efficiency to trichloroethylene (TCE). The regeneration and stability results show that NZVI-immobilized membrane system can be regenerated without obvious performance reduction, which remain the reactivity after half a year storage period.
These results suggest that PAN-based oxidized membrane immobilized with NZVI exhibit significant potential for environmental applications.Chalif, David J2004-12-01The pipes of pan is the crowning achievement of Pablo Picasso's neoclassical period of the 1920s. This monumental canvas depicts a mythological Mediterranean scene in which two sculpted classical giants stare out, seemingly across the centuries, toward a distant and lost Arcadia. Picasso was influenced by Greco-Roman art during his travels in Italy, and his neoclassical works typically portray massive, immobile, and pensive figures. Pan and his pipes are taken directly from Greek mythological lore by Picasso and placed directly into 20th century art. He frequently turned to various mythological figures throughout his metamorphosing periods. The Pipes of Pan was also influenced by the painter's infatuation with the beautiful American expatriate Sara Murphy, and the finished masterpiece represents a revision of a previously conceived neoclassical work.
The Pipes of Pan now hangs in the Musee Picasso in Paris.2013-07-08The shepherd moon Pan orbits Saturn in the Encke gap while the A ring surrounding the gap displays wave features created by interactions between the ring particles and Saturnian moons in this image from NASA Cassini spacecraft.Samadi, Saman; Yazd, Shabnam Sharif; Abdoli, Hossein; Jafari, Pooya; Aliabadi, Majid2017-12-01In the present study, the chitosan (bottom layer)/ polyacrylonitrile (top layer, PAN) nanofibers were coated on the sponge surface. The synthesized magnetic Fe 3 O 4 - ZSM-5 nanozeolites have been loaded into the chitosan/ PAN nanofibers to increase the performance of nanofibers toward absorption of lubricating oil, motor oil and pump oil from water surfaces. Scanning electron microscope (SEM), Transmission electron microscope (TEM) and X-ray diffraction (XRD) analysis were used to characterize the synthesized nanozeolites. The morphology and wettability of nanofibers were determined using SEM and water contact angle tests. The influence of Fe 3 O 4 - ZSM-5 nanozeolite content and chitosan/ PAN/Fe 3 O 4 - ZSM-5 nanofiber thickness was evaluated on the potential of sponges for oils absorption. The maximum capacity of the chitosan/ PAN/Fe 3 O 4 - ZSM-5 nanofibers coated sponges for absorption of motor oil, lubricating oil and pump oil was found to be 99.4, 95.3 and 88.1g/g, in Fe 3 O 4 - ZSM-5 2wt.% and nanofiber thickness of 12μm (chitosan layer of 2μm and PAN layer of 10μm). The reusability of nanofibrous sponges showed that the hydrophobic chitosan/ PAN/Fe 3 O 4 - ZSM-5 nanofibers coated sponges can be easily reused in water-oil separation for many cycles.
Copyright © 2017 Elsevier B.V. All rights reserved.Sheng, Junlu; Xu, Yue; Yu, Jianyong; Ding, Bin2017-05-03Superhydrophobic waterproof-breathable membranes have attracted considerable interest owing to their multifunctional applications in self-cleaning, anti-icing, anticorrosion, outdoor tents, and protective clothing. Despite the researches pertaning to the construction of superhydrophobic functional membranes by nanoparticle finishing have increased drastically, the disconnected particle component is easy to fall off from the membranes under deformation and wear conditions, which has restricted their wide use in practice. Here, robust superhydrophobic microporous membranes were prepared via a facile and environmentally friendly strategy by dip-coating amino-silicone oil (ASO) onto the electrospun polyacrylonitrile ( PAN) membranes, followed by SiO 2 nanoparticles (SiO 2 NPs) blade coating. Compared with hydrophilic PAN membranes, the modified membranes exhibited superhydrophobic surface with an advancing water contact angle up to 156°, after introducing ASO as low surface energy substance and SiO 2 NPs as filler to reduce the pore size and construct the multihierarchical rough structure.
Varying the concentrations of ASO and SiO 2 NPs systematically, the PAN electrospun membranes modified with 1 wt% ASO and 0.1 wt% SiO 2 NPs were endowed with good water-resistance (74.3 kPa), relative low thermal conductivity (0.0028 W m -1 K -1 ), modest vapor permeability (11.4 kg m -2 d -1 ), and air permeability (20.5 mm s -1 ). Besides, the inorganic-organic hybrid coating of ASO/SiO 2 NPs could maintain its superhydrophobicity even after 40 abrasion cycles. The resulting membranes were found to resist variations on the pH scale from 0 to 12, and retained their water repellent properties when exposed to harsh acidic and alkali conditions. This facile fabrication of durable fluorine-free superhydrophobic membranes simultaneous with good waterproof-breathable performance provides the advantages for potential applications in self-cleaning materials and versatile protective.Raghavan, Prasanth; Zhao, Xiaohui; Shin, Chorong; Baek, Dong-Ho; Choi, Jae-Won; Manuel, James; Heo, Min-Yeong; Ahn, Jou-Hyeon; Nah, Changwoon.
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The nodal officer at the top level is a horror though, if you live in Delhi, there is no use contacting the nodal officer of Tata Indicom broadband, he will never solve your queries and keep. @Hari – I dont think you need any driver for the router,it should work plug and play unless u use it as a USB router? Driving towards innovations, the company plans to leverage its product -mobile Internet - to connect with a significant target group, the youth. With the objective of showing off its VAS (value added service) offerings, Tata Indicom has conceptualised and executed an AFP (advertiser's funded programme).
47 sec - Uploaded by pulkitsethUsed condition, up for sale. At ViewItem&item. Tata Indicom Corner, K G Road, Gandhinagar, Bangalore. Get Directions, Location Map, Address, Contact Details, Phone Number, Explore Surroundings, Images, Videos and 360 View for Tata Indicom Corner in Bangalore. It has set up a call centre with trained agents who will offer directions on call and will also send SMSs with driving directions to mobile phones.
More on the launch here. This service is network agnostic and is more mass-market as it does not require any handset upgrade.
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Price is the main motivator for close to 39% subscribers while Network Quality is main driver to 36% of subscribers. Promotion, Reputation/ Recommendation and Customer Service were. Ifyou face really serious problems (eg in connection with a driving accident), contact your consular office as quickly as possible.
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A brand known for many firsts, Idea was the first to launch GPRS and EDGE. I assume you are using a Tata Indicom Photon EVDO connection. They use a ZTE AC8710 USB modem device.The apple WWAN drivers work prefectly for this, but the default driver list does not include the vendor and device ID for this particular device, so the system is unable to recognize the ZTE device.
I have been using TATA Photon + for over a month now and so I thought that it would be nice to share my views about TATA Indicom's Mobile Broadband service – TATA Photon +. When you insert the Photon+ in your PC or Laptop USB slot it installs all the necessary softwares and drivers automatically. Jobs 1 - 10 of 19. 19 Customer Care Executive Job For Vodafone, Aircel, Airtel, Tata Indicom Jobs available in Chennai, Tamil Nadu on Indeed.co.in. Tata Indicom Exclusive Store Panipat City Guide. Tata Indicom Exclusive Store Panipat City, Panipat City Guide, Colleges, Schools, Hotels, Mobiles Dealers, Jobs in Panipat, Map and Pincode.
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Tata Docomo eKYC enables existing customer re-verification as well as onboarding and subsequent activation for a new Tata Docomo customer. The app helps make both processes paperless, fast and efficient by relying on the customer's Aadhaar unique identification number (UID) and biometric (fingerprint). Choose continue and also choose the country from which you are making the connection( INDIA in your case) and select the provider from the list of providers (TATA INDICOM (Photon+) and click continue. Finally choose apply and connect the USB Modem and wait for about 5 minutes to allow network. The process of getting the Tata Photon Plus is simple.
Just visit the nearest Tata Indicom center and ask for the Photon Plus broadband USB device. You need to submit one id proof ( your driving licence or Passport), one address proof (electricity / credit card / landline bill) and one photo.
Once you submit. Here are the drivers for the TATA Photon ZTE AC 8710 USB Modem. Although the drivers. The driver works fine with Windows 7, Vista, XP etc and can also be used with the ZTE AC 8700 which is provided by BSNL for their EVDO Data Card. Download Now. How difficult it was to get Tata Indicom dialer. TATA Indicom (Tele Service), 25.
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We are the dealers for Tata Docomo, Tata Indicom and Virgin Mobiles.Pre-paid and post-paid connections, Mobile handsets, USB Modem and Wireless data cards, Wireless phones, Landline phones, Walky and Tata Indicom Recharge Cards are available here. Q/ what networks work at Rainforest house? A/ vodafone, tata indicom and tata docomo work ok but airtel does not work. Q/ do you offer accommodation for drivers? A/ no we do not have any accommodation for drivers, they usually go back to Tapovan and find accommodation there. Q/ can rafting be arranged? Explore and share the best Tata Nano GIFs and most popular animated GIFs here on GIPHY.
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